Two-Phase Flow Oxidation of Valeraldehyde with O2 in a
Microstructured Reactor
Version 3 2018-02-09, 23:06
Version 2 2017-10-17, 17:50
Version 1 2016-02-12, 09:52
Posted on 2018-02-09 - 23:06
Microstructured
reactors are the ideal device for highly exothermic
reactions. In this work, the highly exothermic two-phase reaction
of valeraldehyde with oxygen to valeric acid was carried out in a
microreactor. The used device from one-A Engineering Austria GmbH
is designed for process development and intensification and can be
applied in the scale-up process to small-scale commercial production.
The atom economic oxidation of valeraldehyde is performed at 0 to
40 °C with a catalytic amount of manganese(II) acetate. A continuous
flow oxidation of aldehydes in such reactors can be a safe and beneficial
alternative to commercial batch processes.
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Baumeister, Tobias; Kitzler, Hannes; Obermaier, Klemens; Zikeli, Stefan; Röder, Thorsten (2016). Two-Phase Flow Oxidation of Valeraldehyde with O2 in a
Microstructured Reactor. ACS Publications. Collection. https://doi.org/10.1021/acs.oprd.5b00173
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AUTHORS (5)
TB
Tobias Baumeister
HK
Hannes Kitzler
KO
Klemens Obermaier
SZ
Stefan Zikeli
TR
Thorsten Röder