Synthesis of Functionalized Diaryl Sulfides by Cobalt-Catalyzed
Coupling between Arylzinc Pivalates and Diaryl Disulfides
Version 2 2018-11-16, 18:07
Version 1 2018-11-16, 18:04
Posted on 2018-11-16 - 18:07
An
efficient protocol for the cobalt-catalyzed preparation of diaryl
sulfides from solid organozinc pivalates and commercially available
diaryl disulfides is reported.
This cross-coupling proceeds at room temperature and displays a good
functional group tolerance, allowing the preparation of a diversity
of symmetrical or asymmetrical diaryl sulfides in 60–95% yield.
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Dong, Zhi-Bing; Balkenhohl, Moritz; Tan, Eric; Knochel, Paul (2018). Synthesis of Functionalized Diaryl Sulfides by Cobalt-Catalyzed
Coupling between Arylzinc Pivalates and Diaryl Disulfides. ACS Publications. Collection. https://doi.org/10.1021/acs.orglett.8b03319
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AUTHORS (4)
ZD
Zhi-Bing Dong
MB
Moritz Balkenhohl
ET
Eric Tan
PK
Paul Knochel