Rubidium and Cesium Enediamide Complexes Derived from
Bulky 1,4-Diazadienes
Posted on 2020-07-24 - 00:13
The first rubidium
and cesium enediamide complexes based on bulky
1,4-diaza-1,3-diene ligands (DADs) have been prepared by metalation
of either 1,4-bis(2,6-diisopropylphenyl)-1,4-diaza-1,3-butadiene (1, = H2DADDipp) or 1,4-bis(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene
(2, = Me2DADDipp) with an excess
of Rb or Cs metals in coordinating solvents such as tetrahydrofuran
(THF) or 1,2-dimethoxyethane (DME). All new complexes were fully characterized
by spectroscopic and analytical methods as well as single-crystal
X-ray diffraction studies.
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Duraisamy, Ramesh; Liebing, Phil; Harmgarth, Nicole; Lorenz, Volker; Hilfert, Liane; Feneberg, Martin; et al. (2020). Rubidium and Cesium Enediamide Complexes Derived from
Bulky 1,4-Diazadienes. ACS Publications. Collection. https://doi.org/10.1021/acsomega.0c02414
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AUTHORS (9)
RD
Ramesh Duraisamy
PL
Phil Liebing
NH
Nicole Harmgarth
VL
Volker Lorenz
LH
Liane Hilfert
MF
Martin Feneberg
RG
Rüdiger Goldhahn
FE
Felix Engelhardt
FE
Frank T. Edelmann