Rhodium-Catalyzed Cycloadditions between 3‑Diazoindolin-2-imines
and 1,3-Dienes
Posted on 2017-03-29 - 21:19
Azepino[2,3-b]indoles
were regioselectively prepared
through rhodium-catalyzed formal aza-[4 + 3] cycloaddition between
3-diazoindolin-2-imines and 1,3-dienes in moderate to good yields.
Using 2-[(trimethylsilyl)oxy]-1,3-butadiene as the diene component,
azepino[2,3-b]indol-4(1H)-ones were
constructed. Furthermore, the reactions of cyclic dienes, such as
1,3-cyclohexadiene and 1,3-cyclopentadiene, furnished the corresponding
[3 + 2] cycloaddition products.
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Lang, Bo; Zhu, Huangtianzhi; Wang, Chen; Lu, Ping; Wang, Yanguang (2017). Rhodium-Catalyzed Cycloadditions between 3‑Diazoindolin-2-imines
and 1,3-Dienes. ACS Publications. Collection. https://doi.org/10.1021/acs.orglett.7b00438
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AUTHORS (5)
BL
Bo Lang
HZ
Huangtianzhi Zhu
CW
Chen Wang
PL
Ping Lu
YW
Yanguang Wang