Rapid Determination of Enantiomeric Excess via NMR
Spectroscopy: A Research-Informed Experiment
Posted on 2016-09-30 - 17:54
An undergraduate chemistry experiment
that draws from primary research
is described. The experiment exploits chiral supramolecular assemblies
for the determination of enantiomeric excess by 1H NMR
spectroscopy. This report describes the delivery of the experiment
to a cohort of students, and as a result of feedback from those involved,
an optimized protocol is presented. Particular care has been taken
to facilitate ready adoption in other institutions by providing comprehensive
teaching support materials as well as technical guidance for supporting
the experiment.
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Fossey, John S.; Anslyn, Eric V.; Brittain, William
D. G.; Bull, Steven D.; Chapin, Brette M.; S. Le Duff, Cécile; et al. (2016). Rapid Determination of Enantiomeric Excess via NMR
Spectroscopy: A Research-Informed Experiment. ACS Publications. Collection. https://doi.org/10.1021/acs.jchemed.6b00355
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AUTHORS (13)
JF
John S. Fossey
EA
Eric V. Anslyn
WB
William
D. G. Brittain
SB
Steven D. Bull
BC
Brette M. Chapin
CS
Cécile S. Le Duff
TJ
Tony D. James
GL
Glenn Lees
SL
Stephanie Lim
JL
Jennifer
A. C. Lloyd
CM
Charles V. Manville
DP
Daniel T. Payne
KR
Kimberley A. Roper