Palladium-Catalyzed Ullmann Cross-Coupling of β‑Iodoenones
and β‑Iodoacrylates with o‑Halonitroarenes
or o‑Iodobenzonitriles and Reductive Cyclization
of the Resulting Products To Give Diverse Heterocyclic Systems

Carr, Paul D.

Palladium-Catalyzed Ullmann Cross-Coupling of β‑Iodoenones and β‑Iodoacrylates with o‑Halonitroarenes or o‑Iodobenzonitriles and Reductive Cyclization of the Resulting Products To Give Diverse Heterocyclic Systems

Posted on 2018-04-20 - 16:21

The palladium-catalyzed Ullmann cross-coupling of β-iodoenones and β-iodoacrylates such as 5 (X = I) with o-halonitroarenes and o-iodobenzonitriles including 2 affords products such as compound 7. These can be engaged in a range of reductive cyclization reactions leading to heterocyclic frameworks such as 3,4-benzomorphan derivative 43.

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Khan, Faiyaz; Dlugosch, Michael; Liu, Xin; Khan, Marium; Banwell, Martin G.; Ward, Jas S.; et al. (2018). Palladium-Catalyzed Ullmann Cross-Coupling of β‑Iodoenones and β‑Iodoacrylates with o‑Halonitroarenes or o‑Iodobenzonitriles and Reductive Cyclization of the Resulting Products To Give Diverse Heterocyclic Systems. ACS Publications. Collection. https://doi.org/10.1021/acs.orglett.8b01015

https://doi.org/10.1021/acs.orglett.8b01015

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