Palladium-Catalyzed Three-Component Coupling of Ynamides

Yoshimura, Yuichi

Palladium-Catalyzed Three-Component Coupling of Ynamides

Posted on 2020-06-26 - 21:06

A palladium-catalyzed regioselective three-component coupling of ynamides was developed. The reaction proceeded smoothly to furnish the desired products when carried out at 70 °C in acetonitrile/water with potassium carbonate in the presence of 2.5 mol % Pd₂(dba)₃·CHCl₃ without a ligand. Various iodides and boronic acids were used in this reaction, and a carbon–carbon bond was formed with satisfactory regioselectivity from the ynamides.

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Wakamatsu, Hideaki; Takahashi, Ayano; Ishii, Ayaka; Kikuchi, Youhei; Sasaki, Madoka; Saito, Yukako; et al. (2020). Palladium-Catalyzed Three-Component Coupling of Ynamides. ACS Publications. Collection. https://doi.org/10.1021/acs.orglett.0c01426

https://doi.org/10.1021/acs.orglett.0c01426

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