Palladium-Catalyzed [5 + 2] Cycloaddition of Vinyloxiranes
with Sulfamate-Derived Cyclic Imines To Construct 1,3-Oxazepine Heterocycles
Posted on 2017-11-18 - 20:30
Palladium-catalyzed [5 + 2] cycloaddition
of 2-aryl-2-vinyloxiranes
with sulfamate-derived cyclic imines is described. The zwitterionic
allylpalladium intermediates act as five-membered synthon to react
with sulfamate-derived cyclic imines to furnish [5 + 2] cycloaddition,
giving 1,3-oxazepine derivatives in moderate to excellent yields with
excellent regioselectivities.
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Wu, Yang; Yuan, Chunhao; Wang, Chang; Mao, Biming; Jia, Hao; Gao, Xing; et al. (2017). Palladium-Catalyzed [5 + 2] Cycloaddition of Vinyloxiranes
with Sulfamate-Derived Cyclic Imines To Construct 1,3-Oxazepine Heterocycles. ACS Publications. Collection. https://doi.org/10.1021/acs.orglett.7b02704
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AUTHORS (11)
YW
Yang Wu
CY
Chunhao Yuan
CW
Chang Wang
BM
Biming Mao
HJ
Hao Jia
XG
Xing Gao
JL
Jianning Liao
FJ
Feng Jiang
LZ
Leijie Zhou
QW
Qijun Wang
HG
Hongchao Guo