Environmental Transmission Electron Microscopy (ETEM)
Studies of Single Iron Nanoparticle Carburization in Synthesis Gas
Version 2 2017-06-23, 18:22
Version 1 2017-06-23, 18:18
Posted on 2017-06-23 - 18:22
Structural
evolution of iron nanoparticles involving the formation
and growth of iron carbide nuclei in the iron nanoparticle was directly
visualized at the atomic level, using environmental transmission electron
microscopy (TEM) under reactive conditions mimicking Fischer–Tropsch
synthesis. Formation of the iron carbide nuclei and surface reconstruction
of the iron nanoparticle play an essential role in carburization of
the iron nanoparticle and consequent formation of Fe5C2. Identification of carbide and oxide intermediates evidenced
by high-resolution TEM images, electron diffraction patterns and electron
energy-loss spectra provides a detailed picture from initial activation
to final degradation of iron under synthesis gas.
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Liu, Xi; Zhang, Chenghua; Li, Yongwang; Niemantsverdriet, J. W.; Wagner, Jakob B.; Hansen, Thomas W. (2017). Environmental Transmission Electron Microscopy (ETEM)
Studies of Single Iron Nanoparticle Carburization in Synthesis Gas. ACS Publications. Collection. https://doi.org/10.1021/acscatal.7b00946
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AUTHORS (6)
XL
Xi Liu
CZ
Chenghua Zhang
YL
Yongwang Li
JN
J. W. Niemantsverdriet
JW
Jakob B. Wagner
TH
Thomas W. Hansen