Alkylamination of Styrenes with Alkyl N‑Hydroxyphthalimide Esters and Amines by B(C6H5)3‑Facilitated Photoredox Catalysis

Li, Jin-Heng

Alkylamination of Styrenes with Alkyl N‑Hydroxyphthalimide Esters and Amines by B(C₆H₅)₃‑Facilitated Photoredox Catalysis

Posted on 2018-10-19 - 20:33

A new, three-component 1,2-alkylamination of styrenes with alkyl N-hydroxyphthalimide (NHP) esters and amines by Lewis acid and visible-light photoredox cooperative catalysis is described. This reaction employs alkyl NHP esters as general alkylation reagents to accomplish the 1,2-alkylamination of alkenes in high efficiency and with excellent functional groups tolerance, significantly enhancing the synthetic potential of 1,2-alkylaminations of alkenes for accessing complex functionalized amines.

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Ouyang, Xuan-Hui; Li, Yang; Song, Ren-Jie; Li, Jin-Heng (2018). Alkylamination of Styrenes with Alkyl N‑Hydroxyphthalimide Esters and Amines by B(C₆H₅)₃‑Facilitated Photoredox Catalysis. ACS Publications. Collection. https://doi.org/10.1021/acs.orglett.8b02670

https://doi.org/10.1021/acs.orglett.8b02670

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