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3,3'-Dichloro-4,5-dimethoxy-biphenyl Information.pdf (340.42 kB)
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3,3'-Dichloro-4,5-dimethoxy-biphenyl 1HNMR spectrum.pdf (70.21 kB)
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3,3'-Dichloro-4,5-dimethoxy-biphenyl GC-MS spectrum.pdf (63.75 kB)
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3,3'-Dichloro-4,5-dimethoxy-biphenyl 1HNMR raw.rar (393.81 kB)
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Authentication of 3,3'-dichloro-4,5-dimethoxy-biphenyl

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posted on 2019-06-24, 17:25 authored by Ram DhakalRam Dhakal, Chun-Yun Zhang, Susanne Flor, Patricia Ruiz, Lynn M. Teesch, Gabriele Ludewig, Hans-Joachim LehmlerHans-Joachim Lehmler
3,3'-Dichloro-4,5-dimethoxy-biphenyl is a derivative of PCB 11 (3,3'-dichlorobiphenyl) and was synthesized as an analytical standard to study the metabolism of PCB 11, a polychlorinated biphenyl (PCB) congener that is not present in technical PCB mixtures. This compound was synthesized via Suzuki cross coupling of 5-bromo-3-chloro-1,2-dimethoybenzene and 3-chlorophenylboronic acid.

Funding

ES027169

ES013661

ES005605

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    Keywords

    authentication3,3'-dichlorobiphenylPCB 11polychlorinated biphenyls (PCBs)Superfund chemicalsmethoxy PCBOrganic Chemical SynthesisOrganic ChemistryToxicology

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