Fig_3.tif (1016.28 kB)

Plate-transfer of ³H-D3 in TLC matrices.

figure

posted on 2015-06-05, 04:52 authored by Nan Jiang, Leonie H. E. Leithold, Julia Post, Tamar Ziehm, Jörg Mauler, Lothar Gremer, Markus Cremer, Elena Schartmann, N. Jon Shah, Janine Kutzsche, Karl-Josef Langen, Jörg Breitkreutz, Dieter Willbold, Antje Willuweit

A control experiment was performed by placing a new TLC plate to a freshly developed plate to transfer only the ³H-D3 within matrices. On the mirror image of the transferred plate, the ³H signals at the start points as well as the smears were obviously reduced, while the intensity of separated ³H-D3 did only change slightly. This result suggests that the observed artefacts arise from unspecific ³H-D3 binding to the glass surface.