Direct
Covalent Coupling of Porphyrins to Graphene
Version 3 2018-08-01, 08:18
Version 2 2017-11-09, 05:44
Version 1 2017-08-21, 13:43
Posted on 2018-08-01 - 08:18
Graphene–porphyrin
nanohybrid materials with a direct covalent
linkage between the graphene carbon network and the functional porphyrin
unit have been successfully synthesized via a one-pot reductive diazotation
approach. A graphite–potassium intercalation compound (KC8) was dispersed in THF, and different isolated porphyrin–diazonium
salts were added. The direct covalent binding and the detailed characterization
of the functional hybrid material were carried out by Raman spectroscopy,
TG-MS, UV/vis, and fluorescence spectroscopy. LDI-ToF mass spectrometry
was introduced as a new versatile and sensitive tool to investigate
covalently functionalized graphene derivatives and to establish the
composition of the respective nanohybrid materials.
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Dasler, Daniela; Schäfer, Ricarda A.; Minameyer, Martin B.; Hitzenberger, Jakob F.; Hauke, Frank; Drewello, Thomas; et al. (2017). Direct
Covalent Coupling of Porphyrins to Graphene. ACS Publications. Collection. https://doi.org/10.1021/jacs.7b04122
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AUTHORS (7)
DD
Daniela Dasler
RS
Ricarda A. Schäfer
MM
Martin B. Minameyer
JH
Jakob F. Hitzenberger
FH
Frank Hauke
TD
Thomas Drewello
AH
Andreas Hirsch