lsyc_a_1382535_sm7740.doc (1.74 MB)
One-pot synthesis of cinnamic anhydrides from cinnamic acids and 6-chloro-2,4-dimethoxy-sec-triazine (CDMT) at room temperature
Version 2 2017-11-30, 21:31
Version 1 2017-10-09, 14:00
journal contribution
posted on 2017-11-30, 21:31 authored by Gabriel Charles Edwin Raja, Yujeong Son, Myungjin Kim, Sunwoo Lee, Jonghoon OhSymmetric cinnamic anhydrides were prepared by the reactions of cinnamic acid substrates with 6-chloro-2,4-dimethoxy-sec-triazine. The reactions were performed at room temperature for 15 h. Diverse cinnamic acid substrates bearing electron-withdrawing or -donating groups worked well, providing the corresponding cinnamic anhydrides in moderate-to-good yields