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LM-1_intermediate_final_Mass spec.pdf (93.74 kB)

I-LM-1_crude_intermediate_mass_spec

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posted on 2016-09-08, 09:33 authored by Andrew MarshAndrew Marsh, Lingcong Meng, Julie V MacPherson

Mass spectrum of crude product from treatment of dec-9-en-1-ylisocyanate (Curtius rearrangement product) with trifluoroacetic acid. After aqueous workup. Note expected m/z for molecular ion not seen.

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