%0 Generic %A Dhakal, Ram %A Zhang, Chun-Yun %A Flor, Susanne %A Ruiz, Patricia %A Teesch, Lynn M. %A Ludewig, Gabriele %A Lehmler, Hans-Joachim %D 2019 %T Authentication of 3,3'-dichloro-4,5-dimethoxy-biphenyl %U https://figshare.com/articles/dataset/Authentication_of_3_3_-dichloro-4_5-dimethoxy-biphenyl/8269832 %R 10.6084/m9.figshare.8269832.v1 %2 https://ndownloader.figshare.com/files/15534980 %2 https://ndownloader.figshare.com/files/15462038 %2 https://ndownloader.figshare.com/files/15462041 %2 https://ndownloader.figshare.com/files/15462362 %2 https://ndownloader.figshare.com/files/15462107 %2 https://ndownloader.figshare.com/files/15462104 %2 https://ndownloader.figshare.com/files/15462359 %K authentication %K 3,3'-dichlorobiphenyl %K PCB 11 %K polychlorinated biphenyls (PCBs) %K Superfund chemicals %K methoxy PCB %K Organic Chemical Synthesis %K Organic Chemistry %K Toxicology %X 3,3'-Dichloro-4,5-dimethoxy-biphenyl is a derivative of PCB 11 (3,3'-dichlorobiphenyl) and was synthesized as an analytical standard to study the metabolism of PCB 11, a polychlorinated biphenyl (PCB) congener that is not present in technical PCB mixtures. This compound was synthesized via Suzuki cross coupling of 5-bromo-3-chloro-1,2-dimethoybenzene and 3-chlorophenylboronic acid.
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