10.1021/acs.orglett.8b02904.s001 Valentina M. Breising Valentina M. Breising Tile Gieshoff Tile Gieshoff Anton Kehl Anton Kehl Vincent Kilian Vincent Kilian Dieter Schollmeyer Dieter Schollmeyer Siegfried R. Waldvogel Siegfried R. Waldvogel Electrochemical Formation of 3,5-Diimido-1,2-dithiolanes by Dehydrogenative Coupling American Chemical Society 2018 diimido electrochemical electrolysis setup access derivative approach Electrochemical Formation dithioanilide Diimido Dehydrogenative precursor cyclic disulfide moiety yield 2018-10-15 18:23:41 Journal contribution https://acs.figshare.com/articles/journal_contribution/Electrochemical_Formation_of_3_5-Diimido-1_2-dithiolanes_by_Dehydrogenative_Coupling/7209575 A synthetic approach to the cyclic disulfide moiety of 3,5-diimido-1,2-dithiolane derivatives starting with readily available precursors including the electrochemical coupling of dithioanilides is developed. The electrochemical key step provides sustainable synthetic access in high yields, using a very simple electrolysis setup.