10.1021/acs.orglett.8b02904.s001
Valentina
M. Breising
Valentina
M.
Breising
Tile Gieshoff
Tile
Gieshoff
Anton Kehl
Anton
Kehl
Vincent Kilian
Vincent
Kilian
Dieter Schollmeyer
Dieter
Schollmeyer
Siegfried R. Waldvogel
Siegfried R.
Waldvogel
Electrochemical Formation of 3,5-Diimido-1,2-dithiolanes
by Dehydrogenative Coupling
American Chemical Society
2018
diimido
electrochemical
electrolysis setup
access
derivative
approach
Electrochemical Formation
dithioanilide
Diimido
Dehydrogenative
precursor
cyclic disulfide moiety
yield
2018-10-15 18:23:41
Journal contribution
https://acs.figshare.com/articles/journal_contribution/Electrochemical_Formation_of_3_5-Diimido-1_2-dithiolanes_by_Dehydrogenative_Coupling/7209575
A synthetic
approach to the cyclic disulfide moiety of 3,5-diimido-1,2-dithiolane
derivatives starting with readily available precursors including the
electrochemical coupling of dithioanilides is developed. The electrochemical
key step provides sustainable synthetic access in high yields, using
a very simple electrolysis setup.