%0 Journal Article %A Guiry, Kevin P. %A Coles, Simon J. %A Moynihan, Humphrey A. %A Lawrence, Simon E. %D 2008 %T Effect of 1-Deoxy-d-lactose upon the Crystallization of d-Lactose %U https://acs.figshare.com/articles/journal_contribution/Effect_of_1_Deoxy_d_lactose_upon_the_Crystallization_of_d_Lactose/2902792 %R 10.1021/cg070598n.s002 %2 https://ndownloader.figshare.com/files/4600936 %K crystal structure %K Crystallization %K additive %K crystallization %K pattern %K powder data %K synthesis %K formation %K analysis %K room temperature %X The synthesis and crystal structure of 1-deoxy-d-lactose is described, as is its use as an additive in the crystallization of d-lactose. This has resulted in the formation of αβ-d-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns. %I ACS Publications