%0 Journal Article %A Ibis, Cemil %A Ozkok, Funda %D 2016 %T The synthesis and spectral characterization of novel nitrodiene compounds from thiols %U https://tandf.figshare.com/articles/journal_contribution/The_synthesis_and_spectral_characterization_of_novel_nitrodiene_compounds_from_thiols/2064555 %R 10.6084/m9.figshare.2064555 %2 https://ndownloader.figshare.com/files/3671577 %K 1,3-Butadiene %K thioester %K thiols %K single-crystal %K N,S-substituted nitrodienes %X

Novel S-, S,S- and S,O-substituted nitrodiene compounds were synthesized from the reactions of 2-nitro-pentachloro-1,3-butadiene (1) and various thiols in different solvent media. The N,S-substituted nitrodienes also were achieved by the reactions of S-substituted nitrodienes with using morpholine, piperidine and piperazine derivatives. All of the new compounds were characterized by elemental analysis, UV-VIS, FT-IR, 1H-NMR, NMR and mass spectroscopy.

%I Taylor & Francis