10.6084/m9.figshare.2064555
Cemil Ibis
Cemil
Ibis
Funda Ozkok
Funda
Ozkok
The synthesis and spectral characterization of novel nitrodiene compounds from thiols
Taylor & Francis Group
2016
1,3-Butadiene
thioester
thiols
single-crystal
N,S-substituted nitrodienes
2016-01-18 13:31:22
Journal contribution
https://tandf.figshare.com/articles/journal_contribution/The_synthesis_and_spectral_characterization_of_novel_nitrodiene_compounds_from_thiols/2064555
<p>Novel S-, S,S- and S,O-substituted nitrodiene compounds were synthesized from the reactions of 2-nitro-pentachloro-1,3-butadiene <b>(1)</b> and various thiols in different solvent media. The N,S-substituted nitrodienes also were achieved by the reactions of S-substituted nitrodienes with using morpholine, piperidine and piperazine derivatives. All of the new compounds were characterized by elemental analysis, UV-VIS, FT-IR, <sup>1</sup>H-NMR, NMR and mass spectroscopy.</p>